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Sieve Testing: Standards, Certification & Calibration

 were not significantly better than those
Sieving in its most elemental definition achieved by using Mid-Point Sieves.
is the separation of fine material from Mesh-Certified Sieves, Mid-Point Sieves,
coarse material by means of a meshed or and sieves carrying the Manufacturing
perforated surface. The technique was Conformance Certificate are all made with
used as far back as the early Egyptian mesh that already conforms to official
days as a way to size grains. These early standards. However, there are three lower
sieves were made of woven reeds and grade levels of sieve mesh available when
grasses. Today the sieve test is the tolerance levels are not as stringent.
technique used most often for analyzing The first is Market Grade. These sieves
particle-size distribution. have a weave that uses a larger diameter
Although at first look the sieving wire resulting in a high strength
process appears to be elementary, in square-mesh cloth suitable for general
practice, there is a science and art purpose screening. There are no official
involved in producing reliable and standards for Market Grade test sieves.
consistent results. In order to better The second, Mill Grade, is a class of
understand sieving, there are several woven mesh using smaller wire, which
areas of sieve specifications that should results in larger open areas in the
to be explained, including: screen mesh. There is also a Twill Weave
1. What Are Test Sieves? in which the weft and warp wires
Test sieves are measuring devices used to alternatively run over and under two
determine the size and size distribution wires rater than over and under alternate
of particles in a material sample using wires as in standard mesh. As none of
wire mesh of different openings to these have official standards against
separate particles of different sizes. which to measure the expected
Test sieves usually consist of wire mesh performance, none of these are provided
held in a frame. In most laboratory with a mesh certificate.
applications the frame is round and is 5. Sieve Calibration
made from stainless steel or brass. The Quality control of the sieving process is
standard frame sizes are three, six, essential, and for people involved in
eight, ten, or twelve inch diameters and material processing and particle
metric equivalents. The woven mesh can be characterization, sieve calibration can
made of stainless steel, brass, or be a confusing topic. It is beneficial to
bronze. For most applications stainless understand what sieve calibration is, why
steel is the most common material used. a working sieve should be calibrated, and
2. What Are the Limitations of the Test how to calibrate a sieve.
Sieve Procedure? A. What Is Sieve Calibration?
The main limitation with the construction Sieve calibration is the process of
of test sieves is the inherent nature of checking a working sieve's performance.
a woven product including control of sag (A working sieve is a test sieve that is
when mounted and the uniformity of used regularly to perform a particle size
construction of the holding frame. It is analysis.)
also essential to maintain consistent B. Why Calibrate a Working Sieve?
sizing across all the openings in a piece Since working sieves are used daily for
of mesh. tests, they are also cleaned regularly.
Because of the inherent variations of Although frequent use in itself can cause
openings in any woven product there are changes in mesh openings, much of the
limitations to the degree of uniformity damage sustained to working sieves occurs
achieved in the opening size across the during cleaning. Often, the operator
mesh in a sieve. This results in a hurries to clear the mesh of residual
practical limit to the range of openings particles by strongly tapping the frame.
and to the precision of results from a This tapping can distort the mesh.
specific sieve. Operators also use brushes to remove
The sieve test requires particles to pass residual particles after a test. This
through the sieve mesh. The practical process often distorts sections of the
limit for using a test sieve procedure is sieve mesh. These alterations of the
a particle size of 20? (microns). sieve will change the results obtained in
3. What Are the Test Sieve Standards? subsequent tests, hence the need for
The first sieve testing standards were calibration.
developed by W.S. Tyler Company before Excessive damage such as tears or large
1920. This original work predated any distortions of the mesh weave can be
published activity by the standards detected by visual inspection. Damaged
organizations and the Tyler designation sieves can be taken out of service when
is the de facto standard in many the damage is observed. When the change
industries. In 1925, ASTM International is small, visual observation may not
prepared the official standard for Test detect a variation in the test results
Sieve Size, Test Sieve Construction, and attributable to the sieve's change. A way
Test Sieve Mesh in the United States. to determine if changes have occurred is
European Standards were developed by a to compare the sieve's performance
German university group in 1977 and are against a known standard. This is sieve
known by the designation DIN 4188. These calibration.
were followed by British Standards (BS In addition, in operations with tight
410). The International Standards (ISO particle size specifications, calibration
565) were developed by the International of new test sieves is performed to
Standards Organization in Europe. This establish a performance baseline for the
was designed to be the universal sieve.
international standard. However, in C. How is a Test Sieve Calibrated?
practice, all of the standards are in The base point of a sieve calibration
operation. process is the use of a fixed standard
Sieve testing standards relate to the and there are a number of approaches
construction of the sieve frame and mesh used. The most common is the use of a
mounting as well as the tolerances master stack of sieves, a master sample,
allowed in the variability of mesh or calibration spheres or beads.
openings. Basic principles are common to A master stack of sieves includes one of
all of the standards and variations in each of the sieves used in the processes.
terminology and in details are small. A master stack should consist of
These small differences, however, can Mesh-Certified sieves. In the event of
often lead to confusion. The following is tight tolerances for the sieve tests it
a synopsis of the principles behind these is recommended that Mid-Point sieves be
standards. used. The following steps are used for
Test sieve frame standards include the this method:
following: 1. Prepare two samples of the material
1. Rigid construction selected for the calibrations process
2. Cloth (mesh) mounted without 2. Place the master stack of sieves on a
distortion, looseness, or waviness sieve shaker
3. Joint between mesh and frame to be 3. Load one of the samples into the top
filled or constructed so that particles sieve
will not be trapped 4. Run on a sieve shaker for the
4. Frame will be of non-corrosive predetermined time
material and seamless 5. Prepare a percent-retained analysis of
5. Bottom of the frame sized to easily the result
slide into the top of same sized sieve, 6. Place the stack of working sieves
thus enabling stacking (sieves with sizes to match master stack)
6. Cloth opening to be a minimum of 0.5 7. Repeat steps three through five for
inches less than nominal diameter the second sample of the material
The wire cloth (mesh) standards include 8. Compare the results of the two
the following list of nominal size analyses
openings in inches, millimeters 9. Check variance from the master stack
(microns), and sieve number. The against acceptable tolerances
following specific dimensional examples 10. Replace the working sieves that are
come from the ASTM E11 Standard: out of tolerance
1. Permissible variation of average Some users only calibrate one sieve at a
openings (depending on opening size and time and compare it to one sieve from the
ranges from ± 2.9% of nominal size for master set. This procedure can be done
125 mm mesh to ± 15% for 20? mesh) before putting new working sieves in
2. Not more than 5 % of the openings can service.
exceed 1.04 times the nominal size for In some processes master samples are
125 mm mesh to 1.45 times the nominal maintained of all material that is
opening for 20? mesh subject to sieve testing. The results
3. Maximum individual opening (for any expected from working sieves were
opening) ranges from 1.0472 times the established through the use of a master
nominal size for 125 mm mesh to 1.75 sieve stack or other calibration
times the normal mesh for 20? mesh techniques. In this method a sample from
4. Wire diameters are specified and range the master is used and the following
from 8 mm for 125 mm mesh to 0.020 steps are taken:
millimeters for 20? mesh 1. Place the stack of working sieves to
More recently, methods based on laser and be checked on a sieve shaker
energy technologies, sedimentation 2. Load the selected sample from the
techniques, image analysis, and master sample into the top sieve
centrifuge-type methods have gained 3. Run the sieve shaker for the
acceptance. However, procedures using predetermined time
test sieves are still widely used. The 4. Prepare a percent retained analysis of
sieve-test result remains the basis or the result
standard against which newer techniques 5. Compare the results to acceptable
are checked. In addition, the equipment tolerances for the sieves in this stack
cost for the test sieve procedure is 6. Replace the working sieves that are
significantly lower than the capital out of tolerance
investment needed for newer methods. The used sample may be returned to the
4. What Are Sieve Certifications? original master sample. Depending on the
Sieve certifications are statements that type of material, deterioration may occur
a test sieve meets or exceeds published during the sieve test. Where this occurs
criteria. It is an assurance that a new the test sample is discarded after use.
sieve will perform in a predictable way. As with the use of a master stack, some
The closer the tolerance required in a users only calibrate one sieve at a time
manufacturing process, the higher the and compare it to a performance tolerance
level of certification needed. Similarly, chart for that sieve size. This procedure
a master set of test sieves against which can also be used for new working sieves
working sieves (sieves in everyday use) before putting them into service.
are checked for wear and predicted Calibration spheres, in sizes for each of
performance need a high level of the sieves to be calibrated, are used to
certification. When test sieves are part determine the actual results obtained by
of a process that is required to meet each sieve tested. This method is simple
traceability prerequisites, such as a and gives a precise result on the mean
specific ISO level, a certification will aperture size. The result is traceable to
document the needed traceability. NIST and NPL standards. It is a good
Many sieve manufacturers provide a check for standards reporting and for
certificate which states that the sieve setting internal standards. The procedure
was manufactured in conformance with a for this calibration is as follows:
specific standard (e.g., ASTM, ISO). This 1. Select the sieve to be calibrated
Manufacturing Conformance Certificate 2. Empty the contents of the bottle
does not reference nor does it certify containing the appropriate standard onto
conformance of the mesh. Most the sieve
manufacturers supplying a Conformance 3. Shake evenly over the surface for one
Certificate will analyze the mesh and minute
provide a mesh certification for an extra 4. Calculate the percent passing through
charge. and read the mean aperture for a
A Mesh-Certified Sieve will be provided calibration graph
with a certificate that states the sieve The method specified by ASTM is to
was manufactured in accordance with a optically inspect a sample of the
specified standard and it was submitted openings, measure the apertures and the
for laboratory analysis and is certified wire, and compare the results with the
to conform to that specific specification ASTM E11 Standard. Traditionally, this
standard (e.g., ASTM, ISO). has been accomplished visually using a
There is a third level of tolerance which microscope. However, there are new
certifies that the manufacturing standard computer-based image analysis systems
is met and that the mesh was submitted that are beginning to have limited use
for laboratory analysis. It also for sieve calibration.
certifies that its openings fall in the 6. Summary
middle of the specific standard Sieves have a long history as the base
specification (e.g., ASTM, ISO). This is for measuring and analyzing particle size
effectively a 30% better tolerance than in material. In spite of the advent of
the mesh of a Fully-Certified sieve. This new technology-based methods, procedures
is known as a Mid-Point Sieve. These based on sieves continue to be the main
three levels of sieve certification basis for particle size determination. In
enable the comparability of performance order to produce reliable and consistent
of one sieve to another of the same size. results, it is evident that sieving
Until the development of the Mid-Point requires an understanding of not just
Sieve, high levels of comparability were one, but a combination of integral
achieved by providing sieves that were factors such as test sieves, limitations
optically matched to a user's standard of the test sieve procedure, test sieve
sieve. A time consuming and costly standards, sieve certifications, and
procedure was needed to accomplish this sieve calibration.
level of comparability and the results




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